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Ultrasound irradiation of hydrothermally engineered sub-20 nm PbS nanoparticles and effect of their size on Aspergillus species morphology

Research Abstract

Lead sulfide nanoparticles were hydrothermally synthesized
and their size was diminished via exposure to ultrasound
waves. Both h-PbS and h,us-PbS nanoparticles of
different sizes were characterized using powder X-ray
diffraction, TEM microscopy and surface area measurements.
The nanoparticles limited the growth of Aspergillus
pathogens and light microscopy proved severe morphological
abnormalities in the fungal vesicles, conidiophores and
mycelia in response to the nanoparticles.

Research Authors
Ghada Abd-Elmonsef Mahmoud and Ahmed B.M. Ibrahim
Research Date
Research Journal
Mendeleev Communications
Research Pages
93–96
Research Publisher
ELSIEVER
Research Rank
International
Research Vol
34
Research Website
https://scholar.google.com.eg/scholar?oi=bibs&cluster=7246516611154290990&btnI=1&hl=en
Research Year
2024

New strategies for sterilization and preservation of fresh fish skin grafts

Research Abstract

The introduction of fish skin as a biological dressing for treating burns and wounds holds great
promise, offering an alternative to existing management strategies. However, the risk of disease
transmission is a significant concern. Therefore, this study aimed to examine how established
sterilization and preservation procedures affected fish skin grafts’ microbiological and histological
properties for long‑term usage. Lyophilization of the fish skin graft followed by rehydration in
normal saline for 15 min did not change the collagen content. Furthermore, gamma irradiation of
the lyophilized fish skin graft at different lengths 5, 10, and 25 KGy showed a significant reduction in
microbial growth (aerobic bacteria, aerobic yeasts, and fungi) at 15‑ and 30 days after the irradiation.
However, exposure to 10 KGy was found to be the most effective intensity among the different
gamma irradiation lengths since it preserved the collagen fiber content and intensity in the lyophilized
fish skin grafts at 15‑ and 30 days after the irradiation. These findings provide efficient preservation
and sterilization methods for long‑term usage of the fresh Tilapia skin grafts used for biological
dressings.

Research Authors
Ahmed Ibrahim 1*, Hossam M. Fahmy 2 , Ghada Abd‑Elmonsef Mahmoud 3 , Mahmoud Soliman 4,5 & Abdelnaby M. Elshahawy
Research Date
Research Journal
Scientific Reports
Research Pages
1253
Research Publisher
@ Springer
Research Rank
International Q1
Research Vol
14
Research Year
2024

Metal-organic frameworks (MOFs)-derived ZrOSO4@C for photocatalytic synthesis of benzimidazole derivatives

Research Abstract

Heterocyclic moieties, such as benzimidazole, are examples of important nuclei that have found widespread use in a variety of scientific subfields, such as medical and applied chemistry. In this study, we described the photocatalytic synthesis of numerous different benzimidazole derivatives using a solid-state acid composed of zirconium oxosulfate embedded into carbon (ZrOSO4@C). A metal-organic framework (MOF), known as UiO-66, was used as a precursor for the synthesis of ZrOSO4@C via carbonization in the presence of sulfuric acid. ZrOSO4@C was able to catalyze the reaction effectively, allowing for a condensation and cyclization to take place in a single vessel, which resulted in a high yield (77–98%) of benzimidazoles that were of high purity with the byproducts of water, and hydrogen (H2) gas. Our catalyst allowed for an improvement in the synthesis of many different benzimidazole derivatives by …

Research Authors
Hani Abdelhamid, Islam Mekhemer, Abdel-Aal Gaber
Research Date
Research Department
Research Journal
Molecular Catalysis
Research Pages
113418
Research Publisher
Elsevier
Research Year
2023

Chitosan-cellulose nanocomposite: Preparation, characterization, and evaluation as cationic color precipitant in sugar clarification process

Research Abstract

The present paper aims to use natural biodegradable polymers of chitosan (CS) and cellulose (CEL) to synthesize green chitosan-cellulose (CS-CEL) nanocomposite as a new clarifying agent. This is the cutting-edge of the sugar industry's clarification process. The CS-CEL nanocomposite showed outstanding results in zeta potential analysis, with a maximum value (+) 57.73 mV, leading to remarkable results in color adsorption via electrostatic attraction. It was also observed that CS-CEL has high mechanical stability. When CS and CS-CEL nanocomposite were used in the clarification of sugarcane (MJ), the findings demonstrated an improvement in color removal of up to 8.7% using CS and 18.1% using CS-CEL nanocomposite compared to currently phosphotation clarification process. Also, Turbidity decreased using CS-CEL nanocomposite compared to the traditional phosphotation clarification process. Overall …

Research Authors
Ahmed S. Ibrahim, Ahmed N. Gad, Hemat M. Dardeer, Abdel-Aal M. Gaber
Research Date
Research Department
Research Journal
Food Chemistry
Research Year
2023

Novel green biodegradable clarifying agents in sugar refining process using functionalized chitosan nanocomposites

Research Authors
Ahmed S Ibrahim, Ahmed N Gad, Hemat M Dardeer, Abdel-Aal M Gaber
Research Date
Research Department
Research Journal
Sustainable Materials and Technologies
Research Publisher
Elsevier
Research Vol
35
Research Year
2023

A review: Zinc oxide nanoparticles: advantages and disadvantages

Research Abstract

Nanomaterials (NMs) have distinctive physicochemical characteristics and offer adaptable scaffolds for biomolecule functionalization. NMs have such a wide range of properties and use that a general evaluation of their health and environmental concerns is impossible. A necessary component of sustainable development is the application of nanotechnology (NT) research in the agricultural sector. The green revolution and new farming techniques have significantly increased crop yield but gradually reduced soil micronutrients, including Zn, Mo, and Fe. It is possible to employ NT to increase the availability of micronutrients for plants. The significant interests of using NT in agriculture include specific applications like nano-fertilizers and nano-pesticides to trail products and nutrient levels to increase productivity without contamination of soils and waters and protection against several insect pests and microbial …

Research Authors
Afaf M Hamada, Abeer A Radi, Fatma A Al‑Kahtany, Fatma A Farghaly
Research Date
Research Journal
Journal of Plant Nutrition
Research Pages
1-24
Research Publisher
Taylor & Francis
Research Year
2023

Carbon dots for electrochemical analytical methods

Research Abstract

Carbon dots (CDs) with small particles less than 10 nm offered unique electrochemical properties. They can be synthesized via various methods using abundant carbon sources. The electrochemical properties of CDs can be optimized via several strategies, including doping with heteroatoms, optimizing the synthesis conditions, and postsynthetic procedures. CDs can be used as suitable electron transporters. They exhibit several advantages, such as a large surface area that offers simple electrode fabrication and enables a high contact area with the investigated analyte. The electrochemical properties of CDs have advanced the analysis of different analytes, including heavy metals ions, biomarkers, hydrogen peroxide, drugs, and other species. The functional groups of CDs provided strong interactions with the vast number of analytes promoting direct electron transfer. CDs offered high sensitivity, good selectivity, and promising properties for analyzing real samples.

Research Authors
Hani Nasser Abdelhamid
Research Date
Research Department
Research Journal
Carbon Dots in Analytical Chemistry Detection and Imaging
Research Member
Research Pages
77-86
Research Publisher
Elsevier
Research Website
https://www.sciencedirect.com/science/article/abs/pii/B9780323983501000232
Research Year
2023

Carbon dots-based fluorescence spectroscopy for metal ion sensing

Research Abstract

Carbon dots (CDs) have been used as a fluorescence probe to sense heavy metal ions. They can be synthesized using cheap sources and offer good optical properties. They provide good photoluminescence properties. The fluorescence emission of CDs can be tuned by controlling particle size, selecting suitable excitation wavelength, and changing the chemical composition via doping with heteroatoms. The synthesis procedure can also affect the optical properties of the synthesized CDs. The unique optical emission enables the sensing of heavy metals, including biological heavy metals (e.g., Fe3+, Zn2+, Cu2+) and toxic metals (e.g., Pb2+, As3+, Ag+, ClO). CDs as fluorescence probes enable a low detection limit and a good linear relationship for a wide concentration range. They can be applied for actual samples with promising properties for assembling electronic devices. This book chapter summarizes the applications of CDs as fluorescence probes to detect heavy metal ions.

Research Authors
Hani Nasser Abdelhamid
Research Journal
Carbon Dots in Analytical Chemistry Detection and Imaging
Research Member
Research Pages
87-96
Research Publisher
Elsevier
Research Website
https://www.sciencedirect.com/science/article/abs/pii/B9780323983501000256
Research Year
2023
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