Skip to main content

Novel Method for the Synthesis of s-Triazolo[3,4-b][1,3,4]thiadiazines

Research Abstract
The acid-promoted condensation of the triazole (I) with a variety of ketones results in formation of triazolothiadiazines (III) in good yields.
Research Authors
Hassan A. H. El-Sherief, Zeniab A. Hozien, Ahmed F. M. El-Mahdy, Abdelwareth A. O. Sarhan
Research Department
Research Journal
ChemInform
Research Member
Abdel-wareth Abdel-Halim Othman Sarhan
Research Rank
1
Research Vol
Vol. 41, Issue 48
Research Website
http://onlinelibrary.wiley.com/doi/10.1002/chin.201048161/full
Research Year
2010

Novel Method for the Synthesis of s-Triazolo[3,4-b][1,3,4]thiadiazines

Research Abstract
The acid-promoted condensation of the triazole (I) with a variety of ketones results in formation of triazolothiadiazines (III) in good yields.
Research Authors
Hassan A. H. El-Sherief, Zeniab A. Hozien, Ahmed F. M. El-Mahdy, Abdelwareth A. O. Sarhan
Research Department
Research Journal
ChemInform
Research Rank
1
Research Vol
Vol. 41, Issue 48
Research Website
http://onlinelibrary.wiley.com/doi/10.1002/chin.201048161/full
Research Year
2010

Studies on the Reaction of N-(3-Carbethoxy-4,5,6,7-
tetrahydrobenzo[b]thien-2-yl)-N'-phenylthiourea with Hydrazine
Hydrate (Part 1)

Research Abstract
The reaction of N-(3-carbethoxy-4,5,6,7-tetrahydrobenzo[b]thien-2-yl)-N′-phenylthiourea (1) with hydrazine hydrate in 1-butanol afforded a mixture of compounds 2, 3 and 4. Treatment of 3 and 4 with nitrous acid gave 6 and 8 respectively, while reactions of 3 with acetylacetone gave 7. Synthesis of tetracyclic compounds 9a-f and 11 from the reactions of 3 with ethyl orthoformate or appropriate acids, acid chloride, carbon disulphide and/or ethyl chloroformate. Also its reaction with isothiocyanate derivatives gave the corresponding thiosemicarbzides 12a,b which on, refluxing in alcoholic KOH gave the unexpected tetracyclic products 14a,b. Similarly the tetracyclic compounds 16a-e and 19 were obtained by cyclization of 4 and 18 respectively.
Research Authors
Hassan A. H. El-Sherief, Galal M. El-Naggar, Zeinab A. Hozien and
Suliman M. El-Sawaisi
Research Department
Research Journal
Heterocyclic Chemistry
Research Member
Galal Mostafa ahmed Mousa El-nagar
Research Pages
PP. 467–473
Research Rank
1
Research Vol
Vol. 45, Issue 2
Research Website
http://onlinelibrary.wiley.com/doi/10.1002/jhet.5570450226/abstract?systemMessage=Due+to+system+maintenance%2C+Usage+reports+are+currently+unavailable.
Research Year
2008

Studies on the Reaction of N-(3-Carbethoxy-4,5,6,7-
tetrahydrobenzo[b]thien-2-yl)-N'-phenylthiourea with Hydrazine
Hydrate (Part 1)

Research Abstract
The reaction of N-(3-carbethoxy-4,5,6,7-tetrahydrobenzo[b]thien-2-yl)-N′-phenylthiourea (1) with hydrazine hydrate in 1-butanol afforded a mixture of compounds 2, 3 and 4. Treatment of 3 and 4 with nitrous acid gave 6 and 8 respectively, while reactions of 3 with acetylacetone gave 7. Synthesis of tetracyclic compounds 9a-f and 11 from the reactions of 3 with ethyl orthoformate or appropriate acids, acid chloride, carbon disulphide and/or ethyl chloroformate. Also its reaction with isothiocyanate derivatives gave the corresponding thiosemicarbzides 12a,b which on, refluxing in alcoholic KOH gave the unexpected tetracyclic products 14a,b. Similarly the tetracyclic compounds 16a-e and 19 were obtained by cyclization of 4 and 18 respectively.
Research Authors
Hassan A. H. El-Sherief, Galal M. El-Naggar, Zeinab A. Hozien and
Suliman M. El-Sawaisi
Research Department
Research Journal
Heterocyclic Chemistry
Research Pages
PP. 467–473
Research Rank
1
Research Vol
Vol. 45, Issue 2
Research Website
http://onlinelibrary.wiley.com/doi/10.1002/jhet.5570450226/abstract?systemMessage=Due+to+system+maintenance%2C+Usage+reports+are+currently+unavailable.
Research Year
2008

Synthesis, Characterization and Studies of New 3-Benzyl-4H-1,2,4-
triazole-5-thiol and Thiazolo[3,2-b][1,2,4]triazole-5(6H)-one
Heterocycles

Research Authors
Abdelwareth A. O. Sarhan, Hassan. A. H. ElSherif, Abdalla M. Mahmoud
and Osama M. A. Habib
Research Department
Research Journal
Heterocyclic Chemistry
Research Member
Osama Mahmoud Ali Habib
Research Rank
1
Research Vol
Vol 45,
Research Year
2008

Synthesis, Characterization and Studies of New 3-Benzyl-4H-1,2,4-
triazole-5-thiol and Thiazolo[3,2-b][1,2,4]triazole-5(6H)-one
Heterocycles

Research Authors
Abdelwareth A. O. Sarhan, Hassan. A. H. ElSherif, Abdalla M. Mahmoud
and Osama M. A. Habib
Research Department
Research Journal
Heterocyclic Chemistry
Research Member
Abd Allah Mohamed Mahmoud Ahmed
Research Rank
1
Research Vol
Vol 45,
Research Year
2008

Synthesis, Characterization and Studies of New 3-Benzyl-4H-1,2,4-
triazole-5-thiol and Thiazolo[3,2-b][1,2,4]triazole-5(6H)-one
Heterocycles

Research Authors
Abdelwareth A. O. Sarhan, Hassan. A. H. ElSherif, Abdalla M. Mahmoud
and Osama M. A. Habib
Research Department
Research Journal
Heterocyclic Chemistry
Research Rank
1
Research Vol
Vol 45,
Research Year
2008

Synthesis, Characterization and Studies of New 3-Benzyl-4H-1,2,4-
triazole-5-thiol and Thiazolo[3,2-b][1,2,4]triazole-5(6H)-one
Heterocycles

Research Authors
Abdelwareth A. O. Sarhan, Hassan. A. H. ElSherif, Abdalla M. Mahmoud
and Osama M. A. Habib
Research Department
Research Journal
Heterocyclic Chemistry
Research Member
Abdel-wareth Abdel-Halim Othman Sarhan
Research Rank
1
Research Vol
Vol 45,
Research Year
2008

Finite Dimensional Approximations for Mixed Variational Inequalities with J-Pseudomonotone Operators

Research Abstract
In this paper, we construct and study the convergence of the finite dimensional approximation for the mixed variational inequalities with J-pseudomonotone operators and convex nondifferentiable functionals in real uniformly smooth Banach spaces which admit a weakly sequentially continuous duality map.
Research Authors
A.M. SADDEEK and S. A. AHMED
Research Department
Research Journal
Applied Mathematical Sciences
Research Member
Research Pages
PP. 2867-2874
Research Rank
1
Research Vol
Vol. 2, No. 58
Research Year
2008

Finite Dimensional Approximations for Mixed Variational Inequalities with J-Pseudomonotone Operators

Research Abstract
In this paper, we construct and study the convergence of the finite dimensional approximation for the mixed variational inequalities with J-pseudomonotone operators and convex nondifferentiable functionals in real uniformly smooth Banach spaces which admit a weakly sequentially continuous duality map.
Research Authors
A.M. SADDEEK and S. A. AHMED
Research Department
Research Journal
Applied Mathematical Sciences
Research Pages
PP. 2867-2874
Research Rank
1
Research Vol
Vol. 2, No. 58
Research Year
2008
Subscribe to