A Research team from Chemistry Department, Faculty of Science, Assiut University has succeeded in the oxidation of Methyl Alcohol to Formaldehyde by 97%. This new success has been declared in the Scientific Forum organized by the Centre for Environmental Studies under the title: "Nanomaterials for sustainable Development" under the auspices of Prof. Ahmed A. Gaeis, President of Assiut University in collaboration with the German Habmldot Foudation.